HuagongsheHuagongshe Chemistry Print Report · For research reference only
tert-butyl (3S)-3-aminopyrrolidine-1-carboxylate → HCID 86636257, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | tert-butyl (3S)-3-aminopyrrolidine-1-carboxylate | HCID 854071 | — |
| Reactant | HCID 66897220 | HCID 66897220 | — |
| Product | HCID 86636257 | HCID 86636257 | 47% |
Reaction Steps
The desired compound was prepared according to the procedure of Example B191 step A, using [6-chloro-2,4,8,22-tetraazatetracyclo[14.3.1.1(3,7).1(9,13)]docosa-1(20),3(22),4,6,9(21),10,12,16,18-nonaen-12-yl]methanol trifluoroacetate and tert-butyl (3S)-3-aminopyrrolidine-1-carboxylate as the starting materials in 47% yield. LCMS for C28H34ClN6O2(M+H)+: m/z=521.3.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08871753B2 |
| Source dataset | uspto-grants-2014_10 |
| ORD ID | ord-4a302d8499b2453b8694c70cecd59ca1 |
| Source note | uspto-grants-2014_10 |