Trifluoroacetic acid → HCID 86636290, compound

Participants

Reaction Steps

A solution of tert-butyl {3-[(3-nitrobenzyl)amino]phenyl}carbamate (100 mg, 0.3 mmol) in dichloromethane (3 mL) and trifluoroacetic acid (3 mL) was stirred at 25° C. for 1 h. The reaction mixture was concentrated to a crude residue. This material was purified by preparative LCMS to give the desired product (110 mg, 79%) as a solid. LCMS for C13H14N3O2 (M+H)+: m/z=244.0.

Provenance & Evidence