Phenylacetyl chloride → HCID 86636344, compound

Participants

Reaction Steps

The desired compound was prepared according to the procedure of Example D94 using 6-chloro-N-piperidin-4-yl-2,4,8,18,22-pentaazatetracyclo[14.3.1.1(3,7).1(9,13)]docosa-1(20),3(22),4,6,9(21),10,12,16,18-nonaen-12-amine tris(trifluoroacetate) and benzeneacetyl chloride as the starting materials in 29% yield. LCMS for C30H31ClN7O (M+H)+: m/z=540.2.

Provenance & Evidence