HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-(6-Isocyanatopyridin-2-yl)morpholine → HCID 86636361, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-(6-Isocyanatopyridin-2-yl)morpholine | HCID 18525736 | — |
| Reactant | 6-Chloro-12-(2-piperidin-4-ylethoxy)-2,4,8,18,22-pentaazatetracyclo[14.3.1.1(3,7).1(9,13)]docosa-1(20),3(22),4,6,9(21),10,12,16,18-nonaene tris(trifluoroacetate) | HCID 86636347 | — |
| Product | HCID 86636361 | HCID 86636361 | 45% |
Reaction Steps
The desired compound was prepared according to the procedure of Example D41 using 6-chloro-12-(2-piperidin-4-ylethoxy)-2,4,8,18,22-pentaazatetracyclo[14.3.1.1(3,7).1(9,13)]docosa-1(20),3(22),4,6,9(21),10,12,16,18-nonaene tris(trifluoroacetate) and 4-(6-isocyanatopyridin-2-yl)morpholine as the starting materials in 45% yield. LCMS for C34H39ClN9O3 (M+H)+: m/z=656.2.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08871753B2 |
| Source dataset | uspto-grants-2014_10 |
| ORD ID | ord-720cfc8d4eae47ae95cc94606caece9d |
| Source note | uspto-grants-2014_10 |