2-Phthalimidoethanesulfonyl chloride → HCID 86636381, compound

Participants

Reaction Steps

The desired compound was prepared according to the procedure of Example D20, step A, using 6-chloro-2,4,8,18,22-pentaazatetracyclo[14.3.1.1(3,7).1(9,13)]docosa-1(20),3(22),4,6,9(21),10,12,16,18-nonaen-12-amine tris(trifluoroacetate) and 2-(1,3-dioxo-1,3-dihydro-2H-isoindol-2-yl)ethanesulfonyl chloride as the starting materials in 20% yield. LCMS for C27H23ClN7O4S (M+H)+: m/z=575.9.

Provenance & Evidence