2,4-Difluorobenzoyl chloride → HCID 86636385, compound

Participants

Reaction Steps

The desired compound was prepared according to the procedure of Example D94 using 6-chloro-N-(2-piperidin-4-ylethyl)-2,4,8,18,22-pentaazatetracyclo[14.3.1.1(3,7).1(9,13)]docosa-1(20),3(22),4,6,9(21),10,12,16,18-nonaen-12-amine tetrakis(trifluoroacetate) and 2,4-difluorobenzoyl chloride as the starting materials in 30% yield. LCMS for C31H31ClF2N7O (M+H)+: m/z=590.1.

Provenance & Evidence