HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Fluorobenzenesulphonyl chloride → HCID 86636386, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Fluorobenzenesulphonyl chloride | HCID 137761 | — |
| Reactant | HCID 86636383 | HCID 86636383 | — |
| Product | HCID 86636386 | HCID 86636386 | 50% |
Reaction Steps
The desired compound was prepared according to the procedure of Example D20, step A, using 6-chloro-N-(2-piperidin-4-ylethyl)-2,4,8,18,22-pentaazatetracyclo[14.3.1.1(3,7).1(9,13)]docosa-1(20),3(22),4,6,9(21),10,12,16,18-nonaen-12-amine tetrakis(trifluoroacetate) and 2-fluorobenzenesulphonyl chloride as the starting materials in 50% yield. LCMS for C30H32ClFN7O2S (M+H)+: m/z=608.1.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08871753B2 |
| Source dataset | uspto-grants-2014_10 |
| ORD ID | ord-f5b26f960a4f40ebae8c2364f5ae8181 |
| Source note | uspto-grants-2014_10 |