HuagongsheHuagongshe Chemistry Print Report · For research reference only
5-Methylisoxazole-3-carbonyl chloride → HCID 86636388, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 5-Methylisoxazole-3-carbonyl chloride | HCID 2736894 | — |
| Reactant | HCID 86636389 | HCID 86636389 | — |
| Product | HCID 86636388 | HCID 86636388 | 60% |
Reaction Steps
The desired compound was prepared according to the procedure of Example D94 using 6-chloro-12-(piperidin-4-ylmethoxy)-2,4,8,18,22-pentaazatetracyclo[14.3.1.1(3,7).1(9,13)]docosa-1(20),3(22),4,6,9(21),10,12,16,18-nonaene tris(trifluoroacetate) and 5-methylisoxazole-3-carbonyl chloride as the starting materials in 60% yield. LCMS for C28H29ClN7O3 (M+H)+: m/z=546.2.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08871753B2 |
| Source dataset | uspto-grants-2014_10 |
| ORD ID | ord-872e0532789a45258b54b37e6d14ddb4 |
| Source note | uspto-grants-2014_10 |