Benzyl Bromide → HCID 13882867, compound

Participants

Reaction Steps

A mixture of 6.06 g (0.02 mol) of product of Example 3, 16 g of benzyl bromide, 3 g of potassium carbonate and 50 ml of acetone was held at reflux for 2 hours and concentrated. The residue was treated with water and extracted with ether. The ether solution was dried and concentrated. The residue was kugelrohr distilled at 13 Pa (pot temperature 50° C.) to remove excess benzyl bromide. The residue was crystallized from hexane to give 6.4 g (81%) of product; mp 56°-58.5° C.

Provenance & Evidence