HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethyl naphthalen-2-ylphosphonate → Naphthalene
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethyl naphthalen-2-ylphosphonate | HCID 13569538 | — |
| Reactant | HCID 20209308 | HCID 20209308 | — |
| Product | Naphthalene | HCID 931 | — |
Reaction Steps
Working up is carried out analogously to Example 4 and gives, in addition to 3.3 g of naphthalene, 14.2 g (81%) of a mixture of isomers, dimethylnaphthalene-1-phosphonate (88.8% by area) and dimethylnaphthalene-2-phosphonate (9.7% by area). The current efficiency is 44%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04655883 |
| Source dataset | uspto-grants-1987_04 |
| ORD ID | ord-fb568ba90e5e4b72a4e0a5474eb896d6 |
| Source note | uspto-grants-1987_04 |