HCID 20209285, compound → Biphenyl

Participants

Reaction Steps

After electrolysis, the crude electrolyte contains 3.5% of educt, 27.6% of dimethyl biphenyl-2-phosphonate and 32% of dimethyl biphenyl-4-phosphonate (in % by area), and is worked up analogously to Example 4. Distillation gives 1.25 g of biphenyl and 19.44 g (81%) of a mixture of the products. The current efficiency is 46%.

Provenance & Evidence