HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dibenzylamine → 1-Chloro-3-dibenzylamino-2-propanol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dibenzylamine | HCID 7656 | — |
| Reactant | Epichlorohydrin | HCID 7835 | — |
| Product | 1-Chloro-3-dibenzylamino-2-propanol | HCID 13535479 | 70% |
Reaction Steps
49.3 g (0.25 mol) of dibenzylamine and 25.4 g (0.275 mol) epichlorohydrin are stirred under nitrogen at 85°90° C. for 3 hours. The golden yellow oil obtained is distilled in a high vacuum. 50.5 g (70%) of a colourless oil are obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04656180 |
| Source dataset | uspto-grants-1987_04 |
| ORD ID | ord-e4ccf861c2994c86868556933453c535 |
| Source note | uspto-grants-1987_04 |