HuagongsheHuagongshe Chemistry Print Report · For research reference only
Chloroacetic Acid → HCID 20209923, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Chloroacetic Acid | HCID 300 | — |
| Reactant | Sulfuric Acid | HCID 1118 | — |
| Reactant | Toluene | HCID 1140 | — |
| Reactant | HCID 20209920 | HCID 20209920 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 20209923 | HCID 20209923 | 84.1% |
Reaction Steps
A mixture of 105.6 g (0.5 mole) of N-(2,2-dimethyl-3-hydroxypropyl)dimethylmaleimide, 56.7 g (0.6 mole) of chloroacetic acid, 5.9 g of concentrated sulfuric acid and 400 ml of toluene are heated as described in Example 1 until the formation of water (9 ml) has ceased. The reaction solution is worked up as in Example 1, affording 121 g of a colourless liquid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04656292 |
| Source dataset | uspto-grants-1987_04 |
| ORD ID | ord-4a5aefc07e3c41668223feb25165f639 |
| Source note | uspto-grants-1987_04 |