Chloroacetic Acid → HCID 15919479, compound

HRID 542284Notes

Reaction equation

HRID 542284 reaction equation
[OH:1][CH2:2][CH2:3][O:4][CH2:5][CH2:6][N:7]1[C:11](=[O:12])[C:10]([CH3:13])=[C:9]([CH3:14])[C:8]1=[O:15].[Cl:16][CH2:17][C:18](O)=[O:19].S(=O)(=O)(O)O>C1(C)C=CC=CC=1>[Cl:16][CH2:17][C:18]([O:1][CH2:2][CH2:3][O:4][CH2:5][CH2:6][N:7]1[C:11](=[O:12])[C:10]([CH3:13])=[C:9]([CH3:14])[C:8]1=[O:15])=[O:19]

Participants

5

Reactant 3

HCID 300Chloroacetic AcidHCID 1118Sulfuric AcidHCID 20209921HCID 20209921, compound

Product 1

HCID 15919479HCID 15919479, compound

Reagents, catalysts & solvents 1

HCID 1140TolueneSolvent

Procedure

A mixture of 90.6 g (0.41 mole) of N-(5-hydroxy-3-oxapentyl)dimethylmaleimide, 46.6 g of chloracetic acid, 4.8 g of concentrated sulfuric acid and 400 ml of toluene are reacted and worked up as described in Example 1, affording 112 g of a slightly yellowish liquid.

Workup

  1. customare reacted
  2. customaffording 112 g of a slightly yellowish liquid

Sources & evidence

ORD record
ord-ddd09977b8f1468295ba9f64e5ee6ba4
Source dataset
uspto-grants-1987_04
Patent number
US04656292

Reaction notes

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