Chloroacetic Acid → HCID 15919480, compound

HRID 542285Notes

Reaction equation

HRID 542285 reaction equation
[OH:1][CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][N:8]1[C:12](=[O:13])[C:11]([CH3:14])=[C:10]([CH3:15])[C:9]1=[O:16].[Cl:17][CH2:18][C:19](O)=[O:20].S(=O)(=O)(O)O>C1(C)C=CC=CC=1>[Cl:17][CH2:18][C:19]([O:1][CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][N:8]1[C:12](=[O:13])[C:11]([CH3:14])=[C:10]([CH3:15])[C:9]1=[O:16])=[O:20]

Participants

5

Reactant 3

HCID 300Chloroacetic AcidHCID 1118Sulfuric AcidHCID 20209925HCID 20209925, compound

Product 1

HCID 15919480HCID 15919480, compound

Reagents, catalysts & solvents 1

HCID 1140TolueneSolvent

Procedure

A mixture of 67.6 g (0.30 mole) of N-(6-hydroxyhexyl)dimethylmaleimide, 34.0 g (0.36 mole) of chloroacetic acid, 3.5 g of concentrated sulfuric acid and 300 ml of toluene is reacted and worked up as described in Example 1. The residue consists of 86.6 g of a colourless oil.

Workup

  1. customis reacted

Sources & evidence

ORD record
ord-f9945635da7a4a8aafb7cc7a72f30a58
Source dataset
uspto-grants-1987_04
Patent number
US04656292

Reaction notes

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