HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → Allyloxycarbonylaminoacetyl chloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | N-[(allyloxy)carbonyl]glycine | HCID 11964402 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | Allyloxycarbonylaminoacetyl chloride | HCID 14588174 | — |
Reaction Steps
5.7 ml of thionyl chloride are added at 0° to 3.18 g of allyloxycarbonylaminoacetic acid. At the same temperature, the mixture is then stirred under a protective gas for 2 hours. It is then diluted with absolute toluene and concentrated in a rotary evaporator. IR (CH2Cl2): 3435, 1800, 1725 cm-1.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04656165 |
| Source dataset | uspto-grants-1987_04 |
| ORD ID | ord-21f6f3af9f874a45969ee296760e163c |
| Source note | uspto-grants-1987_04 |