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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 542547Generated: October 31, 2026

N-bromobutanimide → HCID 178526256, compound

https://huagongshe.com/reaction/542547

Reaction equation

Participants

RoleNameHCIDCharge
ReactantN-bromobutanimideHCID 67184—
ReactantHCID 178526257HCID 178526257—
SolventChloroform methanolHCID 21584188—
ProductHCID 178526256HCID 17852625670.5%

Reaction Steps

In this example, 1 m mole of 4-hydroxy-2-(11-hydroxyundecyl) quinoline-N-oxide is dissolved in a liquid mixture of methanol-chloroform (5:1), and 1 m mole of N-bromosuccinimide is added thereto. The mixture is stirred at room temperature for one hour. After the reaction, the solvent is removed therefrom by distillation, and the residue is recrystallized from ethanol, whereby the captioned compound is obtained (yield: 70.5%).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS04657916
Source datasetuspto-grants-1987_04
ORD IDord-e6088231a10a412aa824d59d8e7146e0
Source noteuspto-grants-1987_04