HuagongsheHuagongshe Chemistry Print Report · For research reference only
N-bromobutanimide → HCID 178526256, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N-bromobutanimide | HCID 67184 | — |
| Reactant | HCID 178526257 | HCID 178526257 | — |
| Solvent | Chloroform methanol | HCID 21584188 | — |
| Product | HCID 178526256 | HCID 178526256 | 70.5% |
Reaction Steps
In this example, 1 m mole of 4-hydroxy-2-(11-hydroxyundecyl) quinoline-N-oxide is dissolved in a liquid mixture of methanol-chloroform (5:1), and 1 m mole of N-bromosuccinimide is added thereto. The mixture is stirred at room temperature for one hour. After the reaction, the solvent is removed therefrom by distillation, and the residue is recrystallized from ethanol, whereby the captioned compound is obtained (yield: 70.5%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04657916 |
| Source dataset | uspto-grants-1987_04 |
| ORD ID | ord-e6088231a10a412aa824d59d8e7146e0 |
| Source note | uspto-grants-1987_04 |