HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 542875Generated: October 30, 2026
Ethanol → 4-dimethylamino-N'-(4-nitrophenyl)-benzenecarbohydrazonamide
https://huagongshe.com/reaction/542875
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Ethanol | HCID 702 | — |
| Reactant | Water | HCID 962 | — |
| Reactant | Hydrazine hydrate (1:1) | HCID 24654 | — |
| Reactant | 4-dimethylamino-N-(4-nitrophenyl)-benzenecarbothiamide | HCID 13174864 | — |
| Product | 4-dimethylamino-N'-(4-nitrophenyl)-benzenecarbohydrazonamide | HCID 54028191 | — |
Reaction Steps
A suspension of 30 g of the product of Step A and 180 ml of ethanol was heated to reflux and 30 ml of hydrazine hydrate were added thereto. The mixture was refluxed for 15 minutes and then 180 ml of distilled water were added thereto. The mixture was cooled to 10° C. and was vacuum filtered. The product was washed with water and dried to obtain 19 g of 4-dimethylamino-N'-(4-nitrophenyl)-benzenecarbohydrazonamide melting at 174° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US04659729 |
|---|
| Source dataset | uspto-grants-1987_04 |
|---|
| ORD ID | ord-672695e7844a49fd90d3b7875e88e393 |
|---|
| Source note | uspto-grants-1987_04 |
|---|
