Butylamine → HCID 13907766, compound

Participants

Reaction Steps

1-(anilino)-4-(n-butylamino)-anthraquinone was prepared by reaction of 1-(anilino)-4-tosylanthraquinone with n-butylamine. The isolated and purified reaction product has the structure illustrated below. ##STR15## The yield was 90% and m.p. 118°-120° C. Mass spectrum, m/e 370 (M+), 327 (M-C3H7), 299 (327-CO); 1H-NMR (CD2Cl2)δ12.17 (br s, 1H), 10.78 (br s, 1H), 8.37-8.27 (m, 2H) 7.76-7.39 (m, 4H), 7.33-7.10 (m, 5H), 3.65-3.05 (m, 2H), 1.72-1.38 (m, 4H), 1.07-0.92 (t, 3H); UV/VIS max (Xylenes) 388 nm (ε4000), 598 (14 200), 642 (15 600).

Provenance & Evidence