Water → HCID 86741450, compound

HRID 543103Notes

Reaction equation

HRID 543103 reaction equation
[P:1]([O-])([O:5]CC)[O:2][CH2:3][CH3:4].O.[CH2:10]([O:12][CH2:13][CH2:14][CH2:15][NH2:16])[CH3:11]>C(O)C>[CH2:3]([O:2][P:1]=[O:5])[CH3:4].[CH2:10]([O:12][CH2:13][CH2:14][CH2:15][NH3+:16])[CH3:11]

Participants

5

Reactant 3

HCID 962WaterHCID 22720Propanolamine ethyl etherHCID 3780918Diethylphosphite

Product 1

HCID 86741450HCID 86741450, compoundYield 99.9%

Reagents, catalysts & solvents 1

HCID 702EthanolSolvent2×

Procedure

A mixture of 13.81 g. (0.1 moles) of diethyl phosphite, 20 ml. of water and 20 ml. of ethanol is reacted with a mixture of 10.31 g. (0.1 moles) of 3-ethoxypropyl amine and 30 ml. of ethanol as described in Example 1. 21.3 g. (99.9%) of 3-ethoxypropyl-ammoniumethyl phosphanate are obtained.

Workup

  1. additionA mixture of 13.81 g

Sources & evidence

ORD record
ord-e26b083e837149d791dfdd9bec379288
Source dataset
uspto-grants-1987_04
Patent number
US04661477

Reaction notes

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