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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 543124Generated: October 30, 2026

3-Phenylpropylamine → HCID 14547355, compound

https://huagongshe.com/reaction/543124

Reaction equation

Participants

RoleNameHCIDCharge
Reactant3-PhenylpropylamineHCID 16259—
ReactantN-Benzylaminodiacetic acidHCID 77606—
ProductHCID 14547355HCID 1454735564%

Reaction Conditions

Temperature200 °C

Reaction Steps

3-Phenyl-1-propylamine (3.63 g) and N-benzyliminodiacetic acid (6.0 g) was mixed and heated to 200° C. under a nitrogen atmosphere. The mixture was stirred at this temperature for 1 h, cooled and purified by column chromatography (SiO2, 40°-60° C. petroleum ether/chloroform) to give the title material as a pale orange liquid (5.53 g, 64%).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS04661489
Source datasetuspto-grants-1987_04
ORD IDord-73353220bac14cc592db3ff36f043bf3
Source noteuspto-grants-1987_04