Back
HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 543268Generated: November 1, 2026

Methanol → 1-(3-Phenoxyphenyl)-4-(methoxyphenyl)-4-methyl-1-penten-3-one

https://huagongshe.com/reaction/543268

Reaction equation

Participants

RoleNameHCIDCharge
ReactantMethanolHCID 887—
ReactantPotassium HydroxideHCID 14797—
Reactant3-PhenoxybenzaldehydeHCID 38284—
Reactant3-(4-Methoxyphenyl)-3-methylbutan-2-oneHCID 11127109—
Product1-(3-Phenoxyphenyl)-4-(methoxyphenyl)-4-methyl-1-penten-3-oneHCID 54150540—

Reaction Conditions

Temperature40 °C

Reaction Steps

A mixture of 10 g of 2-(4-methoxyphenyl)-2-methyl-3-butanone, 33.7 g of 3-phenoxybenzaldehyde, 80 ml of methanol and 4.0 g of KOH was stirred at 40° C. for two hours, and then treated in the same manner as described in (a) of (1) of Synthesis Example 1 to give 25 g of 1-(3-phenoxyphenyl)-4-(methoxyphenyl)-4-methyl-1-penten-3-one.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS04661501
Source datasetuspto-grants-1987_04
ORD IDord-2e97adf78e38486fa34ad48e3878c7f0
Source noteuspto-grants-1987_04