Ethanone, 1-(3-phenoxyphenyl)- → 1-[4-(4-Chlorophenyl)-4-methylpentyl]-3-phenoxybenzene
Reaction equation
[CH3:1][C:2]([C:6]1[CH:11]=[CH:10][C:9]([Cl:12])=[CH:8][CH:7]=1)([CH3:5])[CH:3]=O.[CH3:13][C:14]([C:16]1[CH:21]=[CH:20][CH:19]=[C:18]([O:22][C:23]2[CH:28]=[CH:27][CH:26]=[CH:25][CH:24]=2)[CH:17]=1)=O>>[O:22]([C:18]1[CH:17]=[C:16]([CH2:14][CH2:13][CH2:3][C:2]([C:6]2[CH:11]=[CH:10][C:9]([Cl:12])=[CH:8][CH:7]=2)([CH3:5])[CH3:1])[CH:21]=[CH:20][CH:19]=1)[C:23]1[CH:24]=[CH:25][CH:26]=[CH:27][CH:28]=1Participants
3
Procedure
In the same manner as described in Synthesis Example 2, the equivalent mixture of α,α-dimethyl-(4-chlorophenyl)acetaldehyde and 3-phenoxyacetophenone was treated to give 1-(3-phenoxyphenyl)-4-(4-chlorophenyl)-4-methylpentane.
Workup
- customIn the same manner as described in Synthesis Example 2
- additionwas treated
Sources & evidence
- ORD record
- ord-5da334a297af4361a7815865b3ec27e0
- Source dataset
- uspto-grants-1987_04
- Patent number
- US04661501
Reaction notes
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