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Resorcinol → 7-(2,4-Dihydroxyphenyl)-3,7-dimethyloct-1-yl acetate
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Resorcinol | HCID 5054 | — |
| 反応物 | p-Toluenesulfonic acid | HCID 6101 | — |
| 反応物 | Citronellyl Acetate | HCID 9017 | — |
| 溶媒 | Diethyl Ether | HCID 3283 | — |
| 生成物 | 7-(2,4-Dihydroxyphenyl)-3,7-dimethyloct-1-yl acetate | HCID 20206138 | — |
反応手順
11.0 Parts of resorcinol, 10.0 parts of citronellyl acetate and 0.5 parts of p-toluene sulphonic acid are heated at 115° C. for 45 hours. The reaction mixture is then taken up in ether, washed with sodium bicarbonate solution, water, and evaporated. The residual oil is distilled and yields 3.9 parts of 7-(2',4'-dihydroxyphenyl)-3,7-dimethyloct-1-yl acetate b0.2 215° C. with the following percentage composition by weight:
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04661601 |
| 出典データセット | uspto-grants-1987_04 |
| ORD ID | ord-b8b1ed0b9d3a47e191277d737c1ec4a1 |
| 出典メモ | uspto-grants-1987_04 |