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HRID 543308作成日:2026年10月26日

Resorcinol → 7-(2,4-Dihydroxyphenyl)-3,7-dimethyloct-1-yl acetate

https://huagongshe.com/reaction/543308

反応式

関与物質

役割名称HCID仕込み量
反応物ResorcinolHCID 5054—
反応物p-Toluenesulfonic acidHCID 6101—
反応物Citronellyl AcetateHCID 9017—
溶媒Diethyl EtherHCID 3283—
生成物7-(2,4-Dihydroxyphenyl)-3,7-dimethyloct-1-yl acetateHCID 20206138—

反応手順

11.0 Parts of resorcinol, 10.0 parts of citronellyl acetate and 0.5 parts of p-toluene sulphonic acid are heated at 115° C. for 45 hours. The reaction mixture is then taken up in ether, washed with sodium bicarbonate solution, water, and evaporated. The residual oil is distilled and yields 3.9 parts of 7-(2',4'-dihydroxyphenyl)-3,7-dimethyloct-1-yl acetate b0.2 215° C. with the following percentage composition by weight:

情報源と証拠

DOI10.6084/m9.figshare.5104873.v1
特許番号US04661601
出典データセットuspto-grants-1987_04
ORD IDord-b8b1ed0b9d3a47e191277d737c1ec4a1
出典メモuspto-grants-1987_04