HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetone → HCID 13210234, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetone | HCID 180 | — |
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | Sodium Sulfite | HCID 24437 | — |
| Reactant | 5-tert-Butyl-2-methoxybenzene-1-sulfonyl chloride | HCID 13210231 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 13210234 | HCID 13210234 | — |
Reaction Steps
10.7 g (0.04 mol) of 3-(1,1-dimethylethyl)-6-methoxybenzenesulfonyl chloride are introduced into a solution of 15 g of Na2SO3 and 4 g of NaOH in 100 ml of water. After adding a little acetone, the mixture is heated on a steam bath for 30 minutes, then filtered and the pH is adjusted to 2-3 with concentrated hydrochloric acid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04661636 |
| Source dataset | uspto-grants-1987_04 |
| ORD ID | ord-1a3c6204a54e491eba6e9446da57490b |
| Source note | uspto-grants-1987_04 |