HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hexamethylenetetramine → 2-Formyl-4-ethyl-6-methylsulfonylphenol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hexamethylenetetramine | HCID 4101 | — |
| Reactant | Trifluoroacetic acid | HCID 6422 | — |
| Reactant | 2-(Aminomethyl)-4-ethyl-6-(methanesulfonyl)phenol--hydrogen chloride (1/1) | HCID 20206380 | — |
| Product | 2-Formyl-4-ethyl-6-methylsulfonylphenol | HCID 20206386 | — |
Reaction Steps
0.79 g (0.003 mol) of 2-aminomethyl-4-ethyl-6-methylsulfonylphenol hydrochloride is reacted with0.42 g of hexamethylenetetramine in 6 ml of trifluoroacetic acid in analogy to Example 1. Melting point: 114°-116° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04661636 |
| Source dataset | uspto-grants-1987_04 |
| ORD ID | ord-abea08358db64c7ba8d6b99e8ba830d6 |
| Source note | uspto-grants-1987_04 |