HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
4-(3-Methoxyphenyl)but-3-en-2-one → 4-(3-Methoxyphenyl)butan-2-one
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 4-(3-Methoxyphenyl)but-3-en-2-one | HCID 182007 | — |
| Katalysator | Palladium | HCID 23938 | — |
| Lösungsmittel | Methanol | HCID 887 | — |
| Produkt | 4-(3-Methoxyphenyl)butan-2-one | HCID 11423902 | 99,2% |
Reaktionsschritte
A solution of 30.1 g of 4-(3-methoxyphenyl)-3-buten-2-one in 200 ml of MeOH was hydrogenated over 200 mg of 10% palladium on carbon for two hours. The catalyst was filtered and the solvent evaporated in vacuo to give 30.2 g of yellow oily 4-(3-methoxyphenyl)-2-butanone.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US04661635 |
| Quelldatensatz | uspto-grants-1987_04 |
| ORD ID | ord-dddafb513af244f497e8587548727632 |
| Quellennotiz | uspto-grants-1987_04 |