HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 131713500, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 88692580 | HCID 88692580 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | HCID 131713500 | HCID 131713500 | — |
Reaction Steps
1,1-Difluoro-2,5-di-t-butoxycarbonylamino-4-methylene-pentane (3.3 g, 9.4 mmoles) is dissolved in dry ether saturated with hydrogen chloride gas. After standing overnight, the hygroscopic solid obtained is recrystallized twice from methanol/methylene chloride (1.49 g, 71%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04446151 |
| Source dataset | uspto-grants-1984_05 |
| ORD ID | ord-2c1f9b3d915647bfb5986e4ae0c17fd3 |
| Source note | uspto-grants-1984_05 |