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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 543536Generated: October 26, 2026

Dacthal → HCID 70462314, compound

https://huagongshe.com/reaction/543536

Reaction equation

Participants

RoleNameHCIDCharge
ReactantDacthalHCID 2943—
Reactant7-Aminocephalosporanic acidHCID 441328—
ReactantHCID 178521532HCID 178521532—
SolventAcetonitrileHCID 6342—
ProductHCID 70462314HCID 70462314—

Reaction Steps

While utilizing 0.680 g of 7-ACA, 0.900 g of 5-mercapto-2-morpholinocarbonylmethylthio-1,3,4-thiadiazole, 4.0 ml of acetonitrile and 2.70 g of DCPA, the procedure was carried out in accordance with Example 5, and there was obtained 1.02 g (83.3% of yield) of red brown powder of 7-amino-3-[(2-morpholinocarbonylmethylthio-1,3,4-thiadiazol-5-yl)thiomethyl]-3-cephem-4-carboxylic acid.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS04446318
Source datasetuspto-grants-1984_05
ORD IDord-291c79c7964c4fc395677d94a85f454b
Source noteuspto-grants-1984_05