HRID543659
反应详情
EQUATION
反应方程式
REACTANTS
反应物
PRODUCTS
生成物
AUXILIARIES
试剂、催化剂与溶剂
PROCEDURE
实验过程
2-Furfurylamino-5-ethoxycarbonyl-4-hydroxypyrimidine (526 mg, 2 mmol) was hydrolysed in water (10 ml) with NaOH (5 mmol, 200 mg) by refluxing for 3 h. Cooling and acidification to pH 2 yielded the named product as a precipitate. (435 mg, 93% yield).
WORKUP
后处理
- temperatureby refluxing for 3 h
- temperatureCooling
- customacidification to pH 2 yielded the named product as a precipitate