HRID543659

反应详情

EQUATION

反应方程式

HRID 543659 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

2-Furfurylamino-5-ethoxycarbonyl-4-hydroxypyrimidine (526 mg, 2 mmol) was hydrolysed in water (10 ml) with NaOH (5 mmol, 200 mg) by refluxing for 3 h. Cooling and acidification to pH 2 yielded the named product as a precipitate. (435 mg, 93% yield).

WORKUP

后处理

  1. temperatureby refluxing for 3 h
  2. temperatureCooling
  3. customacidification to pH 2 yielded the named product as a precipitate