HuagongsheHuagongshe Chemistry Print Report · For research reference only
Formaldehyde → HCID 178503657, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Formaldehyde | HCID 712 | — |
| Reactant | Methanethiol | HCID 878 | — |
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | quinolin-4-ol | HCID 178516385 | — |
| Solvent | Isopropanol | HCID 3776 | — |
| Product | HCID 178503657 | HCID 178503657 | — |
Reaction Steps
In a similar way to that described in Example 18, 4-hydroxyquinoline was reacted with 40% aqueous formaldehyde and methanethiol in the presence of triethylamine to give the novel 4-hydroxy-3-methylthiomethylquinoline, m.p. 196°-197° (from isopropanol).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04447435 |
| Source dataset | uspto-grants-1984_05 |
| ORD ID | ord-318ecdef19124892a8d2be5a41371b24 |
| Source note | uspto-grants-1984_05 |