5,10-Dihydro-11H-dibenzo(b,e)(1,4)diazepin-11-one → HCID 13285855, compound

HRID 543717Notes

Reaction equation

HRID 543717 reaction equation
[CH:1]1C2C(=O)NC3C=CC=CC=3NC=2C=CC=1.[N:17]1[CH:22]=[CH:21][C:20]([CH2:23][C:24]([N:26]2[C:32]3[CH:33]=[CH:34][CH:35]=[CH:36][C:31]=3[C:30](=[O:37])[NH:29][C:28]3[CH:38]=[CH:39][CH:40]=[CH:41][C:27]2=3)=[O:25])=[CH:19][CH:18]=1>>[CH3:1][N:17]1[CH2:18][CH2:19][C:20]([CH2:23][C:24]([N:26]2[C:32]3[CH:33]=[CH:34][CH:35]=[CH:36][C:31]=3[C:30](=[O:37])[NH:29][C:28]3[CH:38]=[CH:39][CH:40]=[CH:41][C:27]2=3)=[O:25])=[CH:21][CH2:22]1

Participants

3

Reactant 2

HCID 2013275,10-Dihydro-11H-dibenzo(b,e)(1,4)diazepin-11-oneHCID 20460463HCID 20460463, compound2×

Product 1

HCID 13285855HCID 13285855, compound

Procedure

from 5,10-dihydro-11H-dibenzo[b,e][1,4]diazepin-11-one and 4-pyridioacetic acid chloride hydrochloride via 5,10-dihydro-5-[(4-pyridinyl)acetyl]-11H-dibenzo[b,e]-[1,4]diazepin-11-one and 5,10-dihydro-5-[(4-pyridinyl)acetyl]-11H-dibenzo[b,e][1,4]diazepin-11-one methoiodide.

Sources & evidence

ORD record
ord-e75d4dbe79ec48669d5737b4d125b6e8
Source dataset
uspto-grants-1984_05
Patent number
US04447434

Reaction notes

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