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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 543799Generated: October 28, 2026

Hydrogen Sulfide → HCID 23327038, compound

https://huagongshe.com/reaction/543799

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHydrogen SulfideHCID 402—
ReactantTriethylamineHCID 8471—
ReactantHCID 57144111HCID 57144111—
SolventTolueneHCID 1140—
ProductHCID 23327038HCID 23327038—

Reaction Steps

Into a solution of 3-chlorobenzoylamino(ethoxy) acetonitrile (1 g) in toluene (50 ml) containing triethylamine (1 g) was passed hydrogen sulphide gas. The precipitated product (0.72 g) was collected and crystallised from chloroform-light petroleum. m.p. 136°-137°.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS04447446
Source datasetuspto-grants-1984_05
ORD IDord-a54ea18658e5449f97713627b293eeca
Source noteuspto-grants-1984_05