Potassium thiocyanate → HCID 20461213, compound

HRID 543898Notes

Reaction equation

HRID 543898 reaction equation
Cl.[NH2:2][CH:3]([C:7](=[O:10])[CH2:8][CH3:9])[C:4](=O)[CH3:5].[S-:11][C:12]#[N:13].[K+]>O>[CH3:5][C:4]1[NH:13][C:12](=[S:11])[NH:2][C:3]=1[C:7](=[O:10])[CH2:8][CH3:9]

Participants

4

Reactant 2

HCID 516872Potassium thiocyanateHCID 20461222HCID 20461222, compound

Product 1

HCID 20461213HCID 20461213, compound

Reagents, catalysts & solvents 1

HCID 962WaterSolvent

Procedure

Ten grams of 3-amino-2,4-hexanedione hydrochloride are dissolved in 100 ml water. Fifteen grams of potassium thiocyanate are added and the mixture is heated on the steam bath for 10 minutes. On cooling, the title compound is obtained.

Workup

  1. temperaturethe mixture is heated on the steam bath for 10 minutes
  2. temperatureOn cooling

Sources & evidence

ORD record
ord-79402723461a46b89327ce7839d212de
Source dataset
uspto-grants-1984_05
Patent number
US04447619

Reaction notes

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