Acetone → HCID 86738863, compound

Participants

Reaction Steps

A solution of bis-N-acetyl D-cystine (3.2 g) in acetone (30 ml) containing triethylamine (4.0 g) is stirred with allyl bromide (4 ml) for 24 hours. The mixture is diluted with water, washed with 1N sodium hydroxide, 1N hydrochloric acid, brine, dried over sulfate and evaporated to afford bis N-acetyl-D-cystine bis allyl ester. Treatment of this bis compound according to the procedure of Preparation I affords the title compound.

Provenance & Evidence