HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Cyanide → HCID 13326268, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Cyanide | HCID 8929 | — |
| Reactant | HCID 13326267 | HCID 13326267 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 13326268 | HCID 13326268 | — |
Reaction Steps
To 1.35 mmol of 5-bromo-1-(2-methylanilino)-2,4-pyrimidinedione in 5 ml of 50% aqueous ethanol is added 1.41 mmol of sodium cyanide. The mixture is heated to reflux for 4 hours, after which it is cooled to RT, filtered and recrystallized from ethanol to give 6-cyano-1-(2-methylanilino)-2,4-pyrimidinedione.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04448961 |
| Source dataset | uspto-grants-1984_05 |
| ORD ID | ord-c65b9d303e2a47bea721c79a8c27457b |
| Source note | uspto-grants-1984_05 |