HuagongsheHuagongshe Chemistry Print Report · For research reference only
ethanesulfenyl chloride → HCID 13326281, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | ethanesulfenyl chloride | HCID 12275523 | — |
| Reactant | HCID 20459817 | HCID 20459817 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Solvent | Sodium Hydroxide | HCID 14798 | — |
| Product | HCID 13326281 | HCID 13326281 | — |
| Product | HCID 53938821 | HCID 53938821 | — |
Reaction Steps
In the same manner as above, 6-cyano-1-(2,4,6-trichloroanilino)-2,4-pyrimidinedione in aqueous sodium hydroxide is reacted with ethylsulfenyl chloride in methylene chloride, followed by chromatography yields the compounds 6-cyano-3-ethylthio-(2,4,6-trichloroanilino)-2,4-pyrimidinedione and 6-cyano-1-(N-ethylthio-2,4,6-trichloroanilino)-2,4-pyrimidinedione.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04448961 |
| Source dataset | uspto-grants-1984_05 |
| ORD ID | ord-7899167be59b4ff08df6bcbd019a7112 |
| Source note | uspto-grants-1984_05 |