HuagongsheHuagongshe Chemistry Print Report · For research reference only
Pyridine → HCID 53640741, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Pyridine | HCID 1049 | — |
| Reactant | Cyclohexane | HCID 8078 | — |
| Reactant | Diphenylcyclopropenone | HCID 65057 | — |
| Reactant | Quinoxaline, 2-(tribromomethyl)- | HCID 96377 | — |
| Product | HCID 53640741 | HCID 53640741 | — |
Reaction Steps
A solution of one equivalent of 2,3-diphenyl cyclopropenone and two equivalents of 2-tribromomethylquinoxaline in pyridine were heated on a steam bath for five minutes, flooded with cyclohexane and filtered to furnish the crude dye. Chromatography on silica gel furnished a purified sample, λmax =500 nm. A minor product of the reaction obtainedfrom the chromatography was 1-oxo-2,3-diphenyl-7-[bromo(2-quinoxylinyl)methylidene]-7H-indolizine, λmax =600 nm.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04450093 |
| Source dataset | uspto-grants-1984_05 |
| ORD ID | ord-c3f33b3b3bab49089dcc1067cd45b7f5 |
| Source note | uspto-grants-1984_05 |