HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl Salicylate → Methyl 2-(oxiran-2-ylmethoxy)benzoate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl Salicylate | HCID 4133 | — |
| Reactant | Benzenepropanoic acid, 4-hydroxy-, methyl ester | HCID 79706 | — |
| Product | Methyl 2-(oxiran-2-ylmethoxy)benzoate | HCID 279510 | — |
Reaction Steps
The procedure of Example VII for producing methyl 3-[4-(2,3-epoxypropoxy)phenyl]propionate was repeated in all essential details, except methyl salicylate was substituted for methyl 3-(4-hydroxyphenyl)propionate. The boiling point of the product was 148° (p=75μ). The NMR spectrum was consistent with the assigned structure and the elemental analysis with the formula C11H12O4.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04450173 |
| Source dataset | uspto-grants-1984_05 |
| ORD ID | ord-7c375b67a8754ec086113aea157ca7ad |
| Source note | uspto-grants-1984_05 |