Formaldehyde → HCID 86739424, compound

Participants

Reaction Steps

56 g of N-methylolacrylamide were dissolved in 1000 ml of ethanol, then added with 23 ml of ethylacrylate and 0.36 g of dibenzoylperoxide and heated to reflux for 6 hours while stirring under nitrogen atmosphere. After cooling the reaction mixture was poured into acetone under good stirring. The polymer was filtered, washed and dried as usual. Yield: 62 g. Analytical results: free CH2O: absent; total CH2O: 19.10%; [η]: 0.12 dl/g in NaNO3N at 30° C.

Provenance & Evidence