HuagongsheHuagongshe Chemistry Print Report · For research reference only
Bromine → 1-Bromo-4-[(4-chlorophenyl)sulfanyl]-3,3-dimethylbutan-2-one
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Bromine | HCID 24408 | — |
| Reactant | 4-[(4-Chlorophenyl)sulfanyl]-3,3-dimethylbutan-2-one | HCID 12765973 | — |
| Product | 1-Bromo-4-[(4-chlorophenyl)sulfanyl]-3,3-dimethylbutan-2-one | HCID 12765974 | 99% |
Reaction Steps
64 g (0.4 mol) of bromine are added slowly at room temperature to 97 g (0.4 mol) of 1-(4-chlorophenylsulphenyl)-2,2-dimethylbutan-3-one. The reaction mixture is worked up as in Example 1. 127 g (99% of theory) of 1-bromo-4-(4-chlorophenylsulphenyl)-3,3-dimethylbutan-2-one are obtained as a viscous oil. ##STR119##
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04451281 |
| Source dataset | uspto-grants-1984_05 |
| ORD ID | ord-c7c78fe60ef244869ea7242cdd44a9a1 |
| Source note | uspto-grants-1984_05 |