Methanesulfonic Acid → HCID 20458151, compound

Participants

Reaction Conditions

Reaction Steps

A mixture of 50.24 g of bis-(4-phenoxyphenyl)sulfoxide, 140.58 g of anisole and 124.93 g of methane sulfonic acid was heated at 100° C. for 24 hours. The mixture was poured into 700 g of ice water and worked up substantially according to the previously described procedure to give 67.6 g of 4-methoxyphenyl-bis-(4-phenoxyphenyl)sulfonium methane sulfonate (91 percent yield).

Provenance & Evidence