HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzyl Chloride → HCID 20458411, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzyl Chloride | HCID 7503 | — |
| Reactant | 3,7-Dimethyl-3,7-diazabicyclo[3.3.1]nonan-9-ol | HCID 12360832 | — |
| Product | HCID 20458411 | HCID 20458411 | 32.4% |
Reaction Steps
18.3 g of 3,7-dimethyl-3,7-diazabicyclo[3.3.1]nonane-9-ol are reacted with 13.5 g of benzyl chloride for 4 hours at room temperature as described in Example 1. 9 g (32.3%) of 3,7-dimethyl-9-benzyloxy-3,7-diazabicyclo[3.3.1]nonane are obtained; b.p.: 137°-148° C./10 Pa. The free base rapidly crystallizes upon standing; m.p.: 70°-75° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04451473 |
| Source dataset | uspto-grants-1984_05 |
| ORD ID | ord-cf7939750fbe40d691633a1302374290 |
| Source note | uspto-grants-1984_05 |