反应详情

A stirred mixture of ethyl 2-methylbenzoate (30 grams, 0.183 mole) and N-bromosuccinimide (35 grams, 0.194 mole) in carbon tetrachloride (200 ml) was irradiated with an infrared lamp and heated at reflux for 20 minutes. The reaction mixture was allowed to cool to room temperature, then filtered. The filtrate was evaporated under reduced pressure to give ethyl 2-bromomethylbenzoate as a yellow oil.

1. customwas irradiated with an infrared lamp
2. temperatureheated
3. temperatureat reflux for 20 minutes
4. filtrationfiltered
5. customThe filtrate was evaporated under reduced pressure