HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diethyl Ether → HCID 20259244, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diethyl Ether | HCID 3283 | — |
| Reactant | 6,7-dihydro-5H-dibenzo[a,c]cycloheptene-4-carbonyl chloride | HCID 13281342 | — |
| Reactant | Aluminium lithium hydride | HCID 21226445 | — |
| Solvent | Methanol--water (1/1) | HCID 22242641 | — |
| Product | HCID 20259244 | HCID 20259244 | — |
Reaction Steps
The reaction of 6,7-dihydro-5H-dibenzo[a,c]cycloheptene-4-carbonyl chloride (3.5 grams, 0.014 mole), lithium aluminum hydride (0.6 grams, 0.016 mole), and diethyl ether (100 ml) gave a yellow oil. The oil was dissolved in methanol/water, and the solution was extracted with diethyl ether. The extract was dried over anhydrous magnesium sulfate and filtered. The filtrate was evaporated to give 6,7-dihydro-5H-dibenzo[a,c]cycloheptene-4-methanol as a yellow oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04451484 |
| Source dataset | uspto-grants-1984_05 |
| ORD ID | ord-4ceaf7da011d40bf8231fd63cf177680 |
| Source note | uspto-grants-1984_05 |