HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 13281346, compound → HCID 20403339, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 13281346 | HCID 13281346 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 20403339 | HCID 20403339 | 86.4% |
Reaction Steps
The reaction between 5,6,7,8-tetrahydrodibenzo[a,c]cycloocten-4-carboxylic acid (1.7 g, 0.0067 mole) and borane-tetrahydrofuran complex (1.16 g of a 1.05 M solution in tetrahydrofuran) in tetrahydrofuran (50 ml) produced 5,6,7,8-tetrahydrodibenzo[a,c]cycloocten-4-methanol as an oil (1.38 g). The IR and nmr spectra were consistent with the proposed structure.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04451484 |
| Source dataset | uspto-grants-1984_05 |
| ORD ID | ord-e19b7927b2924c158ab4e69a683ba340 |
| Source note | uspto-grants-1984_05 |