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HRID544909

反应详情

EQUATION

反应方程式

HRID 544909 的结构方程式

REACTANTS

反应物

2
结构：O=C(Cl)c1ccc(Br)cc1
HCID68515

Benzoyl chloride, 4-bromo-

C7H4BrClO

结构：CC(=O)OC[C@H]1O[C@@H](n2ccc3c(C)cccc32)[C@H](OC(C)=O)[C@@H](OC(C)=O)[C@@H]1OC(C)=O
HCID67195878

未命名化合物

PRODUCTS

生成物

1
结构：CC(=O)OC[C@H]1O[C@@H](n2cc(Cc3ccc(Br)cc3)c3c(C)cccc32)[C@H](OC(C)=O)[C@@H](OC(C)=O)[C@@H]1OC(C)=O
HCID67197408

未命名化合物

PROCEDURE

实验过程

4-Methyl-1-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)-indole obtained in Example 23-(1) and 4-bromobenzoyl chloride were treated in a manner similar to Example 2-(4), (5) and 3-(3) to give 3-(4-bromophenylmethyl)-4-methyl-1-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)indole as pale pink crystals. mp 190-192° C. APCI-Mass m/Z 630/632 (M+H).