HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl pyruvate → Ethyl 2-(3,5-dichlorophenylhydrazino)propionate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl pyruvate | HCID 12041 | — |
| Reactant | (3,5-Dichlorophenyl)hydrazine monohydrochloride | HCID 2723913 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | Ethyl 2-(3,5-dichlorophenylhydrazino)propionate | HCID 67198185 | — |
Reaction Steps
A mixture of 3,5-dichlorophenylhydrazine hydrochloride (5.07 g) and ethyl pyruvate (3.96 ml) in ethyl alcohol (30 ml) was refluxed for 2 hours, and the solvent was evaporated under reduced pressure. The residual solid was triturated with hexane to give ethyl 2-(3,5-dichlorophenylhydrazino)propionate (5.60 g). APCI-Mass m/Z 275/277 (M+H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07935674B2 |
| Source dataset | uspto-grants-2011_05 |
| ORD ID | ord-b80da5a0e1b448d0b75a6e1f678666ca |
| Source note | uspto-grants-2011_05 |