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HRID544932

反应详情

EQUATION

反应方程式

HRID 544932 的结构方程式

REACTANTS

反应物

2
结构：Cc1c(Br)csc1C(=O)O
HCID2757073

4-Bromo-3-methylthiophenecarboxylic acid

C6H5BrO2S

结构：Cc1ccc(C(=O)NC2CC2)cc1N.Cl
HCID44203194

未命名化合物

PRODUCTS

生成物

1
结构：Cc1ccc(C(=O)NC2CC2)cc1NC(=O)c1scc(Br)c1C
HCID59761512

未命名化合物

PROCEDURE

实验过程

The compound a was prepared by coupling commercially available 4-bromo-3-methylthiophene-2-carboxylic acid with 3-amino-N-cyclopropyl-4-methylbenzamide hydrochloride (prepared as described in WO 04/071440) using the method described in Example 128. HPLC Ret time=3.12 min. LCMS [M+H]+ 393.13.

WORKUP

后处理

  1. customThe compound a was prepared
  2. customHPLC Ret time=3.12 min