HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Pyrrolidinepropanamine → HCID 59851234, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Pyrrolidinepropanamine | HCID 31670 | — |
| Reactant | HCID 59852114 | HCID 59852114 | — |
| Product | HCID 59851234 | HCID 59851234 | — |
Reaction Steps
In a manner similar to that described in Method N, 2-(3,4-dimethoxy-phenylamino)-6-oxo-6,7-dihydro-5H-benzo[b]pyrimido[4,5-d]azepine-10-carboxylic acid (I-43) and 3-(pyrrolidin-1-yl)propan-1-amine were converted to I-77 (6%) after purification by C-18 RP LC-MS chromatography. HRMS Calcd. for C28H32N6O4: 517.2563, Found 517.2552.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07935694B2 |
| Source dataset | uspto-grants-2011_05 |
| ORD ID | ord-949823a7db8f49aa92e076266f3bd390 |
| Source note | uspto-grants-2011_05 |